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SQL FINAL PROGRESS REPORT FEBRUARY 16, 1996
DEPARTMENT OF CHEMISTRY:
Dr. Tamara Leenay
Dr. Alison Johnson
Dr. Donald Neu
PROJECT SUMMARY
The intent of this proposal is to acquire sophisticated, state-of-the-art Fourier
Transformation spectroscopy technology which would be integrated into the
curriculum at St. Cloud State University. To this end, we wish to purchase a modern
Fourier Transform infrared spectrometer with computerized data acquisition and
analysis capabilities, including a spectral data library which students may access to
compare their experimental data with published results. In addition, we wish to
purchase accessories which would allow students to perform sophisticated
experiments which cannot be performed with our current technology.
Answers to questions raised regarding SQL Q7 standards.
1. How did the students assess the experience?
We are still in the preliminary stages of implementation of this new
technology. Two students are actively involved in exploring the multiple
applications of this instrument (see question 9, ÒActivitiesÓ). Both students
eagerly volunteered to participate in these activities. They found the
experience extremely rewarding and appreciated the opportunity to work
with state-of-the-art instrumentation that is an integral technology in both
academic and industrial settings. Many other students have expressed
excitement about the acquisition of this powerful instrumentation and look
forward to the further implementation of this technology into the chemistry
curriculum.
2. How did faculty assess the experience?
During the writing of the proposal, faculty submitted their individual plans for
incorporation of the FTIR into their specific courses. Since then, faculty are
in the process of developing specific experiments/applications for routine
laboratory use. Additionally, five faculty members attended a Nicolet-
sponsored FTIR Training Workshop in Bloomington, MN. Faculty received
essential training in sample preparation, instrumentation operation, and
applications, including microspectroscopy. The workshop gave practical
industrial applications of FTIR as well as basic theory. The faculty found the
workshop to be extremely well-organized and practical.
3. Is on-going discussion across disciplines and between
institutions feasible or desirable?
Not only is it feasible, it is already going on! One student in our department,
Jerry Sykora, is participating in a joint academic/industrial internship with
Champion International (See question 9, ÒActivitiesÓ). In addition, we have
received inquiries from other companies about our willingness to perform
periodic analyses for them using our FTIR microscope. We anticipate
having students performing these analyses to provide them with experience
in industrial problem-solving methods.
4. How was learning affected (method, didactic, and resources) in
the long and short terms?
Learning instrumentation is definitely a hands-on experience! In addition to
traditional instruction by faculty, students also learn by on-screen tutorials,
which enable independent Òself-instructionÓ.
5. How were the objectives of learning affected?
The use of instrumentation in the laboratory brings the theory of chemical
principles into a practical light. Performing analyses will help the students
tie theoretical concepts to real-life chemical problems. We view the use of
instrumentation as a necessary component of applied learning.
6. What are the challenges and benefits of collaborative efforts?
Science, as it is practiced in the real world, is a collaborative effort.
Scientists pool their expertise to solve complex chemical problems. Our
initial proposal was, in fact, a collaborative effort involving the entire
chemistry department, each faculty member having their own perspective on
how this instrumentation would be incorporated into our curriculum. We
view this, not as divisive, but as a way of complementing each others
specialties for the benefit of ourselves and our students. Our joint internship
with Champion International provides students with valuable industrial
experience, and provides Champion with on-going technical support.
Services to other companies in the future may well be self-supporting by
minimal fees or donations.
7. Recommendations and outline for future work
At this point, we, as a faculty, have been in the process of acquiring and
installing the necessary hardware and software, pursuing outside funding,
and earning the basic operation and applications of the instrument. The
next phase is collaboration between faculty members of the chemistry
department in regard to the specific use of the FTIR in the various levels of
the undergraduate curriculum. We intend to expand our collaborative efforts
with the industrial community. The benefits of these collaborative efforts
were outlined in 5 and 6.
8. Budget and Narrative
Q7 funds were used solely for the purchase and installation of the FTIR.
Additional funds were procured to purchase the microspectroscopy system.
(a more complete listing is found under the following question)
9. Give a chronological account of activities, problems, changes,
solutions which pertain to your Q7 grant under SQL.
Activities
¥ The SQL grant was used to purchase the following:
¥Nicolet FTIR spectrometer
¥Gateway computer: data acquisition and instrument operation
¥Color desk jet printer
¥Sample supplies and accessories
Matching funds were used to purchase additional accessories and
equipment.
¥IR microscope and microanalysis accessories
¥ Five Chemistry Department faculty members attended a Nicolet FTIR
Workshop in Bloomington, MN on January 31, 1996 in which they received
training in sampling techniques and microspectroscopy.
¥ One chemistry major, Jerry Sykora, has been participating in a joint
academic/industrial internship for Champion International and the
Chemistry Department at St. Cloud State University. Mr. Sykora collected
chemical samples at Champion, developed a sample preparation protocol,
and cataloged a data base of spectral files for later use by Champion for
purposes of quality control/assurance. Champion will use this data to
troubleshoot manufacturing processes in their paper manufacturing
operations.
¥ Another chemistry major, Rick Schroden, has been participating in an
independent study project involving the creation of an organic compound
data base to be used by students in the Organic Chemistry sequences
291-293 and 251-252.
Problems Encountered
¥ Delay in shipment (IR arrived mid-December 1995, microscope arrived early
January 1996)
¥ Delays in on-site installation and training.
¥ First detector was defective and was replaced under warranty.
¥ Some other minor repairs were necessary.
¥ Difficulties in computer networking.
Changes - none
Solutions - Mechanical and computer difficulties were resolved by the
manufacturers and computer technicians
Which other grants/financial contributions did you get?
Grant Award SQL Q7 25,000.00
Nicolet Academic Equipment Donation 11,565.00
Champion International Paper Company
Equipment Fund Donation 1,500.00
Sponsored Program Matching Funds 13,065.00
Total $51,130.00
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